Validation in Chemical MeasurementPaul De Bièvre, Helmut Günzler Springer Science & Business Media, 2005. gada 6. dec. - 168 lappuses The validation of analytical methods is based on the characterisation of a measurement procedure (selectivity, sensitivity, repeatability, reproducibility). This volume collects 31 outstanding papers on the topic, mostly published in the period 2000-2003 in the journal "Accreditation and Quality Assurance." They provide the latest understanding, and possibly the rationale why it is important to integrate the concept of validation into the standard procedures of every analytical laboratory. In addition, this anthology considers the benefits to both: the analytical laboratory and the user of the measurement results. |
No grāmatas satura
1.–5. rezultāts no 83.
. lappuse
... samples by atomic spectrometry....................................... Validation of test methods. General principles and concepts ......................................... 139 62 Validation requirements for chemical methods ...
... samples by atomic spectrometry....................................... Validation of test methods. General principles and concepts ......................................... 139 62 Validation requirements for chemical methods ...
2. lappuse
... –20 sources of blank samples [4]. Howev- er, in Conference Report II [10], even analysis of only one source of blank matrix was deemed acceptable, if At this point it must be mentioned that the term. 2 F.T. Peters · H.H. Maurer.
... –20 sources of blank samples [4]. Howev- er, in Conference Report II [10], even analysis of only one source of blank matrix was deemed acceptable, if At this point it must be mentioned that the term. 2 F.T. Peters · H.H. Maurer.
3. lappuse
... sample and the corresponding detector response must be investi- gated . This can be done by analysing spiked calibration samples and plotting the resulting responses versus the corresponding concentrations . The resulting standard ...
... sample and the corresponding detector response must be investi- gated . This can be done by analysing spiked calibration samples and plotting the resulting responses versus the corresponding concentrations . The resulting standard ...
4. lappuse
... sampling of the same ho- mogenous sample under the prescribed conditions and may be considered at three levels: repeatability, interme- diate precision and reproducibility [13]. Precision is usu- ally measured in terms of imprecision ...
... sampling of the same ho- mogenous sample under the prescribed conditions and may be considered at three levels: repeatability, interme- diate precision and reproducibility [13]. Precision is usu- ally measured in terms of imprecision ...
5. lappuse
... sample in- dependent from the calibration curve. The advantage of this approach is the fact that the estimation of LLOQ is based on the same quantification procedure used for real samples. LLOQ based on signal to noise ratio (S/N) [12 ...
... sample in- dependent from the calibration curve. The advantage of this approach is the fact that the estimation of LLOQ is based on the same quantification procedure used for real samples. LLOQ based on signal to noise ratio (S/N) [12 ...
Saturs
1 | |
10 | |
Clinical reference materials for the validation of | 31 |
Qualification and validation of software and computer | 42 |
Validation of the uncertainty evaluation for | 63 |
Validation criteria for developing ionselective | 73 |
quality assurance | 148 |
Is the estimation of measurement uncertainty a viable | 155 |
Different approaches to legal requirements | 159 |
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Bieži izmantoti vārdi un frāzes
acceptance Accred Qual Assur accuracy Anal analysis analyte concentration analytical chemistry analytical measurement analytical method analytical procedure Anklam AOAC AOAC INTERNATIONAL application assessment bias calculated calibration curve capillary cation certified certified reference materials Chem chemical clinical components computer systems corrosion criteria CRMs defined detector determination documentation drug EURACHEM evaluation experimental factors functions Hewlett-Packard HPLC injection installation instrument interlaboratory International laboratory linearity LLOQ matrix measurement uncertainty ment meth method validation Metrology mmol/l obtained operating parameters peak performance pharmaceutical phase precision protocol qualification quality assurance quantitative quinizarin range recovery reference materials relative standard deviation reliability reproducibility requirements ruggedness testing sample scope of accreditation solution solvent red 24 solvent yellow 124 specifications Springer-Verlag standard deviation Table tainty test methods tion trueness type of tests uncer uncertainty associated uncertainty estimation vali vendor verification Waldbronn