Validation in Chemical MeasurementPaul De Bièvre, Helmut Günzler Springer Science & Business Media, 2005. gada 6. dec. - 168 lappuses The validation of analytical methods is based on the characterisation of a measurement procedure (selectivity, sensitivity, repeatability, reproducibility). This volume collects 31 outstanding papers on the topic, mostly published in the period 2000-2003 in the journal "Accreditation and Quality Assurance." They provide the latest understanding, and possibly the rationale why it is important to integrate the concept of validation into the standard procedures of every analytical laboratory. In addition, this anthology considers the benefits to both: the analytical laboratory and the user of the measurement results. |
No grāmatas satura
1.–5. rezultāts no 33.
1. lappuse
... recovery and ruggedness (robust- ness). Keywords Method · Validation · Bioanalysis · Toxicology consensus on the extent of validation experiments and on acceptance criteria for validation parameters of bioana- lytical methods in ...
... recovery and ruggedness (robust- ness). Keywords Method · Validation · Bioanalysis · Toxicology consensus on the extent of validation experiments and on acceptance criteria for validation parameters of bioana- lytical methods in ...
2. lappuse
... recovery, reproduc- ibility and ruggedness (robustness) [2, 4–10, 12]. year later, Shah et al. published their report on the con- ference on “Analytical Methods Validation: Bioavailabil- ity, Bioequivalence and Pharmacokinetic Studies ...
... recovery, reproduc- ibility and ruggedness (robustness) [2, 4–10, 12]. year later, Shah et al. published their report on the con- ference on “Analytical Methods Validation: Bioavailabil- ity, Bioequivalence and Pharmacokinetic Studies ...
6. lappuse
... ence samples can be tested against a lower acceptance limit corresponding to 90% of the mean of the compari- son samples [8, 9]. Recovery modifications, where it seems necessary. The definitions established by. 6 F.T. Peters · H.H. Maurer.
... ence samples can be tested against a lower acceptance limit corresponding to 90% of the mean of the compari- son samples [8, 9]. Recovery modifications, where it seems necessary. The definitions established by. 6 F.T. Peters · H.H. Maurer.
7. lappuse
... recovery is not among the validation parameters regarded as essential by the Con- ference Reports. Most authors agree, that the value for recovery is not important, as long as the data for LLOQ, (LOD), precision and accuracy (bias) are ...
... recovery is not among the validation parameters regarded as essential by the Con- ference Reports. Most authors agree, that the value for recovery is not important, as long as the data for LLOQ, (LOD), precision and accuracy (bias) are ...
8. lappuse
... Recovery Recovery does not seem to be a big issue for forensic and clinical toxicologists as long as precision, accuracy (bias), LLOQ and, especially, LOD are satisfactory. However, during method development one should of course try to ...
... Recovery Recovery does not seem to be a big issue for forensic and clinical toxicologists as long as precision, accuracy (bias), LLOQ and, especially, LOD are satisfactory. However, during method development one should of course try to ...
Saturs
1 | |
10 | |
Clinical reference materials for the validation of | 31 |
Qualification and validation of software and computer | 42 |
Validation of the uncertainty evaluation for | 63 |
Validation criteria for developing ionselective | 73 |
quality assurance | 148 |
Is the estimation of measurement uncertainty a viable | 155 |
Different approaches to legal requirements | 159 |
Citi izdevumi - Skatīt visu
Bieži izmantoti vārdi un frāzes
acceptance Accred Qual Assur accuracy Anal analysis analyte concentration analytical chemistry analytical measurement analytical method analytical procedure Anklam AOAC AOAC INTERNATIONAL application assessment bias calculated calibration curve capillary cation certified certified reference materials Chem chemical clinical components computer systems corrosion criteria CRMs defined detector determination documentation drug EURACHEM evaluation experimental factors functions Hewlett-Packard HPLC injection installation instrument interlaboratory International laboratory linearity LLOQ matrix measurement uncertainty ment meth method validation Metrology mmol/l obtained operating parameters peak performance pharmaceutical phase precision protocol qualification quality assurance quantitative quinizarin range recovery reference materials relative standard deviation reliability reproducibility requirements ruggedness testing sample scope of accreditation solution solvent red 24 solvent yellow 124 specifications Springer-Verlag standard deviation Table tainty test methods tion trueness type of tests uncer uncertainty associated uncertainty estimation vali vendor verification Waldbronn