Validation in Chemical MeasurementPaul De Bièvre, Helmut Günzler Springer Science & Business Media, 2005. gada 6. dec. - 168 lappuses The validation of analytical methods is based on the characterisation of a measurement procedure (selectivity, sensitivity, repeatability, reproducibility). This volume collects 31 outstanding papers on the topic, mostly published in the period 2000-2003 in the journal "Accreditation and Quality Assurance." They provide the latest understanding, and possibly the rationale why it is important to integrate the concept of validation into the standard procedures of every analytical laboratory. In addition, this anthology considers the benefits to both: the analytical laboratory and the user of the measurement results. |
No grāmatas satura
1.–5. rezultāts no 20.
5. lappuse
... peaks elute close to the analyte peak. LLOQ based on standard deviation of the response from blank samples [14]. Another definition of LLOQ is the concentration that corresponds to a detector response that is k times greater than the ...
... peaks elute close to the analyte peak. LLOQ based on standard deviation of the response from blank samples [14]. Another definition of LLOQ is the concentration that corresponds to a detector response that is k times greater than the ...
7. lappuse
... peaks. This latter approach is preferable, if the possibly interfering substance is known to be ex- tensively metabolized, as it also allows exclusion of in- terferences from such metabolites, which are usually not available as pure ...
... peaks. This latter approach is preferable, if the possibly interfering substance is known to be ex- tensively metabolized, as it also allows exclusion of in- terferences from such metabolites, which are usually not available as pure ...
9. lappuse
... peak purity) Table 2 Checklist for. Conclusion References 1. Karnes HT , Shiu G , Shah VP ( 1991 ) Pharm Res 8 : 421-426 2. Shah VP , Midha KK , Dighe S , McGilveray IJ , Skelly JP , Yacobi A , Layloff T , Viswanathan CT , Cook CE ...
... peak purity) Table 2 Checklist for. Conclusion References 1. Karnes HT , Shiu G , Shah VP ( 1991 ) Pharm Res 8 : 421-426 2. Shah VP , Midha KK , Dighe S , McGilveray IJ , Skelly JP , Yacobi A , Layloff T , Viswanathan CT , Cook CE ...
11. lappuse
... peak area or peak height) ob- tained from Perkin-Elmer HGA Graphics Software Package with Data System-10. GIRAF program description The operating computer environment is MS-DOS, and the hardware is an IBM-compatible PC. GIRAF reads ...
... peak area or peak height) ob- tained from Perkin-Elmer HGA Graphics Software Package with Data System-10. GIRAF program description The operating computer environment is MS-DOS, and the hardware is an IBM-compatible PC. GIRAF reads ...
12. lappuse
... Peak height Peak area Cu Absorbance Na Emission conc., Prev. New Prev. New conc., Prev. New conc., Prev. New ppb prog. prog. prog. prog. ppm prog. prog. ppm prog. prog. Blank 0.011 0.015 0.006 0.008 Blank 0.000 0.997 Blank P0.004 0.103 ...
... Peak height Peak area Cu Absorbance Na Emission conc., Prev. New Prev. New conc., Prev. New conc., Prev. New ppb prog. prog. prog. prog. ppm prog. prog. ppm prog. prog. Blank 0.011 0.015 0.006 0.008 Blank 0.000 0.997 Blank P0.004 0.103 ...
Saturs
1 | |
10 | |
Clinical reference materials for the validation of | 31 |
Qualification and validation of software and computer | 42 |
Validation of the uncertainty evaluation for | 63 |
Validation criteria for developing ionselective | 73 |
quality assurance | 148 |
Is the estimation of measurement uncertainty a viable | 155 |
Different approaches to legal requirements | 159 |
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Bieži izmantoti vārdi un frāzes
acceptance Accred Qual Assur accuracy Anal analysis analyte concentration analytical chemistry analytical measurement analytical method analytical procedure Anklam AOAC AOAC INTERNATIONAL application assessment bias calculated calibration curve capillary cation certified certified reference materials Chem chemical clinical components computer systems corrosion criteria CRMs defined detector determination documentation drug EURACHEM evaluation experimental factors functions Hewlett-Packard HPLC injection installation instrument interlaboratory International laboratory linearity LLOQ matrix measurement uncertainty ment meth method validation Metrology mmol/l obtained operating parameters peak performance pharmaceutical phase precision protocol qualification quality assurance quantitative quinizarin range recovery reference materials relative standard deviation reliability reproducibility requirements ruggedness testing sample scope of accreditation solution solvent red 24 solvent yellow 124 specifications Springer-Verlag standard deviation Table tainty test methods tion trueness type of tests uncer uncertainty associated uncertainty estimation vali vendor verification Waldbronn