Validation in Chemical MeasurementPaul De Bièvre, Helmut Günzler Springer Science & Business Media, 2005. gada 6. dec. - 168 lappuses The validation of analytical methods is based on the characterisation of a measurement procedure (selectivity, sensitivity, repeatability, reproducibility). This volume collects 31 outstanding papers on the topic, mostly published in the period 2000-2003 in the journal "Accreditation and Quality Assurance." They provide the latest understanding, and possibly the rationale why it is important to integrate the concept of validation into the standard procedures of every analytical laboratory. In addition, this anthology considers the benefits to both: the analytical laboratory and the user of the measurement results. |
No grāmatas satura
1.–5. rezultāts no 43.
2. lappuse
... matrix [1, 2, 4–10, 12, 14]. The requirement estab- lished by the Conference Report [2] to analyse at least six different sources of blank matrix has become state of the art. However, this approach has been subject to criti- cism in the ...
... matrix [1, 2, 4–10, 12, 14]. The requirement estab- lished by the Conference Report [2] to analyse at least six different sources of blank matrix has become state of the art. However, this approach has been subject to criti- cism in the ...
3. lappuse
... matrix . The LLOQ is the lowest amount of an analyte in. hyphenated mass spectrometric methods are used for de- tionships [ 10 ] . However , no information was given on tection . There are only a few principle differences concerning ...
... matrix . The LLOQ is the lowest amount of an analyte in. hyphenated mass spectrometric methods are used for de- tionships [ 10 ] . However , no information was given on tection . There are only a few principle differences concerning ...
5. lappuse
... matrix peaks elute close to the analyte peak. LLOQ based on standard deviation of the response from blank samples [14]. Another definition of LLOQ is the concentration that corresponds to a detector response that is k times greater than ...
... matrix peaks elute close to the analyte peak. LLOQ based on standard deviation of the response from blank samples [14]. Another definition of LLOQ is the concentration that corresponds to a detector response that is k times greater than ...
6. lappuse
... matrix under specific conditions for given time inter- vals” [10]. Stability of the analyte during the whole ana- lytical procedure is a prerequisite for reliable quantifica- tion. Therefore, full validation of a method must include ...
... matrix under specific conditions for given time inter- vals” [10]. Stability of the analyte during the whole ana- lytical procedure is a prerequisite for reliable quantifica- tion. Therefore, full validation of a method must include ...
7. lappuse
... matrix for methods employing MS de- tection does not seem reasonable for toxicological appli- cations because of the great importance of selectivity in this field. However, discussion is needed on how many sources of blank samples ...
... matrix for methods employing MS de- tection does not seem reasonable for toxicological appli- cations because of the great importance of selectivity in this field. However, discussion is needed on how many sources of blank samples ...
Saturs
1 | |
10 | |
Clinical reference materials for the validation of | 31 |
Qualification and validation of software and computer | 42 |
Validation of the uncertainty evaluation for | 63 |
Validation criteria for developing ionselective | 73 |
quality assurance | 148 |
Is the estimation of measurement uncertainty a viable | 155 |
Different approaches to legal requirements | 159 |
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Bieži izmantoti vārdi un frāzes
acceptance Accred Qual Assur accuracy Anal analysis analyte concentration analytical chemistry analytical measurement analytical method analytical procedure Anklam AOAC AOAC INTERNATIONAL application assessment bias calculated calibration curve capillary cation certified certified reference materials Chem chemical clinical components computer systems corrosion criteria CRMs defined detector determination documentation drug EURACHEM evaluation experimental factors functions Hewlett-Packard HPLC injection installation instrument interlaboratory International laboratory linearity LLOQ matrix measurement uncertainty ment meth method validation Metrology mmol/l obtained operating parameters peak performance pharmaceutical phase precision protocol qualification quality assurance quantitative quinizarin range recovery reference materials relative standard deviation reliability reproducibility requirements ruggedness testing sample scope of accreditation solution solvent red 24 solvent yellow 124 specifications Springer-Verlag standard deviation Table tainty test methods tion trueness type of tests uncer uncertainty associated uncertainty estimation vali vendor verification Waldbronn