Validation in Chemical MeasurementPaul De Bièvre, Helmut Günzler Springer Science & Business Media, 2005. gada 6. dec. - 168 lappuses The validation of analytical methods is based on the characterisation of a measurement procedure (selectivity, sensitivity, repeatability, reproducibility). This volume collects 31 outstanding papers on the topic, mostly published in the period 2000-2003 in the journal "Accreditation and Quality Assurance." They provide the latest understanding, and possibly the rationale why it is important to integrate the concept of validation into the standard procedures of every analytical laboratory. In addition, this anthology considers the benefits to both: the analytical laboratory and the user of the measurement results. |
No grāmatas satura
1.–5. rezultāts no 44.
. lappuse
... criteria for developing ion-selective membrane electrodes for analysis of pharmaceuticals .. 73 Analytical procedure in terms of measurement (quality) assurance ................................ 148 Is the estimation of measurement ...
... criteria for developing ion-selective membrane electrodes for analysis of pharmaceuticals .. 73 Analytical procedure in terms of measurement (quality) assurance ................................ 148 Is the estimation of measurement ...
1. lappuse
... criteria for validation pa- rameters. In this review, the most im- portant papers published on this top- ic since 1991 have been reviewed. Terminology, theoretical and practi- cal aspects as well as implications for forensic and ...
... criteria for validation pa- rameters. In this review, the most im- portant papers published on this top- ic since 1991 have been reviewed. Terminology, theoretical and practi- cal aspects as well as implications for forensic and ...
2. lappuse
... criteria for accuracy and precision [3]. Based on their results they questioned the suitability of these criteria for practical application. From 1995 to 1997, ap- plication issues like experimental designs and statistical methods for ...
... criteria for accuracy and precision [3]. Based on their results they questioned the suitability of these criteria for practical application. From 1995 to 1997, ap- plication issues like experimental designs and statistical methods for ...
4. lappuse
... criteria at different levels of precision (repeatability, reproducibility) as RSD under reproducibility conditions is usually considerably greater than under repeatability conditions. Furthermore, if pre- cision and bias estimates are ...
... criteria at different levels of precision (repeatability, reproducibility) as RSD under reproducibility conditions is usually considerably greater than under repeatability conditions. Furthermore, if pre- cision and bias estimates are ...
5. lappuse
... criteria for these two parameters at LLOQ are 20% RSD for precision and ±20% for bias. Only Causon suggested 15% RSD and ±15%, respective- Again, the proposals on how many replicates at each concentration levels should be analysed vary ...
... criteria for these two parameters at LLOQ are 20% RSD for precision and ±20% for bias. Only Causon suggested 15% RSD and ±15%, respective- Again, the proposals on how many replicates at each concentration levels should be analysed vary ...
Saturs
1 | |
10 | |
Clinical reference materials for the validation of | 31 |
Qualification and validation of software and computer | 42 |
Validation of the uncertainty evaluation for | 63 |
Validation criteria for developing ionselective | 73 |
quality assurance | 148 |
Is the estimation of measurement uncertainty a viable | 155 |
Different approaches to legal requirements | 159 |
Citi izdevumi - Skatīt visu
Bieži izmantoti vārdi un frāzes
acceptance Accred Qual Assur accuracy Anal analysis analyte concentration analytical chemistry analytical measurement analytical method analytical procedure Anklam AOAC AOAC INTERNATIONAL application assessment bias calculated calibration curve capillary cation certified certified reference materials Chem chemical clinical components computer systems corrosion criteria CRMs defined detector determination documentation drug EURACHEM evaluation experimental factors functions Hewlett-Packard HPLC injection installation instrument interlaboratory International laboratory linearity LLOQ matrix measurement uncertainty ment meth method validation Metrology mmol/l obtained operating parameters peak performance pharmaceutical phase precision protocol qualification quality assurance quantitative quinizarin range recovery reference materials relative standard deviation reliability reproducibility requirements ruggedness testing sample scope of accreditation solution solvent red 24 solvent yellow 124 specifications Springer-Verlag standard deviation Table tainty test methods tion trueness type of tests uncer uncertainty associated uncertainty estimation vali vendor verification Waldbronn