Validation in Chemical MeasurementPaul De Bièvre, Helmut Günzler Springer Science & Business Media, 2005. gada 6. dec. - 168 lappuses The validation of analytical methods is based on the characterisation of a measurement procedure (selectivity, sensitivity, repeatability, reproducibility). This volume collects 31 outstanding papers on the topic, mostly published in the period 2000-2003 in the journal "Accreditation and Quality Assurance." They provide the latest understanding, and possibly the rationale why it is important to integrate the concept of validation into the standard procedures of every analytical laboratory. In addition, this anthology considers the benefits to both: the analytical laboratory and the user of the measurement results. |
No grāmatas satura
1.–5. rezultāts no 38.
5. lappuse
... calculated mean val- ues at each concentration [6]. If the calculated confi- dence interval includes the accepted true value, one can assume the method to be free of bias at a given level of statistical significance. Another way to test ...
... calculated mean val- ues at each concentration [6]. If the calculated confi- dence interval includes the accepted true value, one can assume the method to be free of bias at a given level of statistical significance. Another way to test ...
6. lappuse
... calculations of LLOQ are basically the same as described under the heading “LLOQ based on standard deviation of the response from the blank samples”. This approach is also applicable for chromatographic meth- ods. Long-term stability ...
... calculations of LLOQ are basically the same as described under the heading “LLOQ based on standard deviation of the response from the blank samples”. This approach is also applicable for chromatographic meth- ods. Long-term stability ...
7. lappuse
... calculated as the percentage of the analyte response after sample workup compared to that Validation parameters of a solution containing the analyte at the theoretical maximum concentration. Therefore, absolute recoveries can usually ...
... calculated as the percentage of the analyte response after sample workup compared to that Validation parameters of a solution containing the analyte at the theoretical maximum concentration. Therefore, absolute recoveries can usually ...
11. lappuse
... calculations are based on the linear regression of data with replicate measurements. If the graphite fur- nace is used, the absorbance peak area and peak height are calculated as the data for regression analysis; if the flame facilities ...
... calculations are based on the linear regression of data with replicate measurements. If the graphite fur- nace is used, the absorbance peak area and peak height are calculated as the data for regression analysis; if the flame facilities ...
12. lappuse
... calculated analyte concentrations in the test solutions Utr described in the Reference materials section are approximately one third of the correspond- ing uncertainties of the results of the analysis (for sodi- um it is not obvious ...
... calculated analyte concentrations in the test solutions Utr described in the Reference materials section are approximately one third of the correspond- ing uncertainties of the results of the analysis (for sodi- um it is not obvious ...
Saturs
1 | |
10 | |
Clinical reference materials for the validation of | 31 |
Qualification and validation of software and computer | 42 |
Validation of the uncertainty evaluation for | 63 |
Validation criteria for developing ionselective | 73 |
quality assurance | 148 |
Is the estimation of measurement uncertainty a viable | 155 |
Different approaches to legal requirements | 159 |
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Bieži izmantoti vārdi un frāzes
acceptance Accred Qual Assur accuracy Anal analysis analyte concentration analytical chemistry analytical measurement analytical method analytical procedure Anklam AOAC AOAC INTERNATIONAL application assessment bias calculated calibration curve capillary cation certified certified reference materials Chem chemical clinical components computer systems corrosion criteria CRMs defined detector determination documentation drug EURACHEM evaluation experimental factors functions Hewlett-Packard HPLC injection installation instrument interlaboratory International laboratory linearity LLOQ matrix measurement uncertainty ment meth method validation Metrology mmol/l obtained operating parameters peak performance pharmaceutical phase precision protocol qualification quality assurance quantitative quinizarin range recovery reference materials relative standard deviation reliability reproducibility requirements ruggedness testing sample scope of accreditation solution solvent red 24 solvent yellow 124 specifications Springer-Verlag standard deviation Table tainty test methods tion trueness type of tests uncer uncertainty associated uncertainty estimation vali vendor verification Waldbronn