Validation in Chemical MeasurementPaul De Bièvre, Helmut Günzler Springer Science & Business Media, 2005. gada 6. dec. - 168 lappuses The validation of analytical methods is based on the characterisation of a measurement procedure (selectivity, sensitivity, repeatability, reproducibility). This volume collects 31 outstanding papers on the topic, mostly published in the period 2000-2003 in the journal "Accreditation and Quality Assurance." They provide the latest understanding, and possibly the rationale why it is important to integrate the concept of validation into the standard procedures of every analytical laboratory. In addition, this anthology considers the benefits to both: the analytical laboratory and the user of the measurement results. |
No grāmatas satura
1.–5. rezultāts no 7.
3. lappuse
... ( LLOQ ) and , if possible , with in- terferents at their highest likely concentrations . In this approach , the method can be considered sufficiently se- lective if precision and accuracy data for these LLOQ samples are acceptable . For ...
... ( LLOQ ) and , if possible , with in- terferents at their highest likely concentrations . In this approach , the method can be considered sufficiently se- lective if precision and accuracy data for these LLOQ samples are acceptable . For ...
4. lappuse
... LLOQ where 20% RSD was accepted. Bias was required to be within ±15% of the accepted true value, except at the LLOQ where ±20% were accepted [2, 10]. These requirements have been subject to criticism in the analysis of the Con- ference ...
... LLOQ where 20% RSD was accepted. Bias was required to be within ±15% of the accepted true value, except at the LLOQ where ±20% were accepted [2, 10]. These requirements have been subject to criticism in the analysis of the Con- ference ...
5. lappuse
... LLOQ. LLOQ based on precision and accuracy (bias) data [2, 7–10, 13, 14]. This is probably the most practical ap- proach and defines the LLOQ as the lowest concentra- tion of a sample that can still be quantified with accept- able ...
... LLOQ. LLOQ based on precision and accuracy (bias) data [2, 7–10, 13, 14]. This is probably the most practical ap- proach and defines the LLOQ as the lowest concentra- tion of a sample that can still be quantified with accept- able ...
6. lappuse
... LLOQ based on standard deviation of the response from the blank samples”. This approach is also applicable for ... LLOQ is by definition not accept- able [2, 5, 9, 10, 13, 14]. Therefore, below this value a method can only produce ...
... LLOQ based on standard deviation of the response from the blank samples”. This approach is also applicable for ... LLOQ is by definition not accept- able [2, 5, 9, 10, 13, 14]. Therefore, below this value a method can only produce ...
7. lappuse
... LLOQ, (LOD), precision and accuracy (bias) are acceptable [1, 5, 7–10]. It can be calculated as the percentage of the analyte response after sample workup compared to that Validation parameters of a solution containing the analyte at ...
... LLOQ, (LOD), precision and accuracy (bias) are acceptable [1, 5, 7–10]. It can be calculated as the percentage of the analyte response after sample workup compared to that Validation parameters of a solution containing the analyte at ...
Saturs
1 | |
10 | |
Clinical reference materials for the validation of | 31 |
Qualification and validation of software and computer | 42 |
Validation of the uncertainty evaluation for | 63 |
Validation criteria for developing ionselective | 73 |
quality assurance | 148 |
Is the estimation of measurement uncertainty a viable | 155 |
Different approaches to legal requirements | 159 |
Citi izdevumi - Skatīt visu
Bieži izmantoti vārdi un frāzes
acceptance Accred Qual Assur accuracy Anal analysis analyte concentration analytical chemistry analytical measurement analytical method analytical procedure Anklam AOAC AOAC INTERNATIONAL application assessment bias calculated calibration curve capillary cation certified certified reference materials Chem chemical clinical components computer systems corrosion criteria CRMs defined detector determination documentation drug EURACHEM evaluation experimental factors functions Hewlett-Packard HPLC injection installation instrument interlaboratory International laboratory linearity LLOQ matrix measurement uncertainty ment meth method validation Metrology mmol/l obtained operating parameters peak performance pharmaceutical phase precision protocol qualification quality assurance quantitative quinizarin range recovery reference materials relative standard deviation reliability reproducibility requirements ruggedness testing sample scope of accreditation solution solvent red 24 solvent yellow 124 specifications Springer-Verlag standard deviation Table tainty test methods tion trueness type of tests uncer uncertainty associated uncertainty estimation vali vendor verification Waldbronn