Quality Assurance in the Analytical Chemistry LaboratoryOxford University Press, 2007. gada 29. marts - 320 lappuses Analytical chemical results touch everyones lives can we eat the food? do I have a disease? did the defendant leave his DNA at the crime scene? should I invest in that gold mine? When a chemist measures something how do we know that the result is appropriate? What is fit for purpose in the context of analytical chemistry? Many manufacturing and service companies have embraced traditional statistical approaches to quality assurance, and these have been adopted by analytical chemistry laboratories. However the right chemical answer is never known, so there is not a direct parallel with the manufacture of ball bearings which can be measured and assessed. The customer of the analytical services relies on the quality assurance and quality control procedures adopted by the laboratory. It is the totality of the QA effort, perhaps first brought together in this text, that gives the customer confidence in the result. QA in the Analytical Chemistry Laboratory takes the reader through all aspects of QA, from the statistical basics and quality control tools to becoming accredited to international standards. The latest understanding of concepts such as measurement uncertainty and metrological traceability are explained for a working chemist or her client. How to design experiments to optimize an analytical process is included, together with the necessary statistics to analyze the results. All numerical manipulation and examples are given as Microsoft Excel spreadsheets that can be implemented on any personal computer. Different kinds of interlaboratory studies are explained, and how a laboratory is judged in proficiency testing schemes is described. Accreditation to ISO 17025 or OECD GLP is nearly obligatory for laboratories of any pretension to quality. Here the reader will find an introduction to the requirements and philosophy of accreditation. Whether completing a degree course in chemistry or working in a busy analytical laboratory, this book is a single source for an introduction into quality assurance. |
No grāmatas satura
1.–5. rezultāts no 32.
viii. lappuse
... certified reference material, are still the subject of intense academic debate. As such, this book runs the risk of being quickly out of date. To avoid this, I have flagged areas that are in a state of flux, and I believe the principles ...
... certified reference material, are still the subject of intense academic debate. As such, this book runs the risk of being quickly out of date. To avoid this, I have flagged areas that are in a state of flux, and I believe the principles ...
14. lappuse
... certified reference materials is designed to establish the traceability chain and its associated measurement uncertainty. Without an internationally agreed-upon anchor (the SI), measurements made around the world in local systems of ...
... certified reference materials is designed to establish the traceability chain and its associated measurement uncertainty. Without an internationally agreed-upon anchor (the SI), measurements made around the world in local systems of ...
46. lappuse
Esat sasniedzis šīs grāmatas aplūkošanas reižu limitu.
Esat sasniedzis šīs grāmatas aplūkošanas reižu limitu.
48. lappuse
Esat sasniedzis šīs grāmatas aplūkošanas reižu limitu.
Esat sasniedzis šīs grāmatas aplūkošanas reižu limitu.
49. lappuse
Esat sasniedzis šīs grāmatas aplūkošanas reižu limitu.
Esat sasniedzis šīs grāmatas aplūkošanas reižu limitu.
Saturs
3 | |
2 Statistics for the Quality Control Laboratory | 23 |
3 Modeling and Optimizing Analytical Methods | 66 |
4 Quality Control Tools | 105 |
5 Interlaboratory Studies | 136 |
6 Measurement Uncertainty | 161 |
7 Metrological Traceability | 203 |
8 Method Validation | 227 |
9 Accreditation | 262 |
Bringing It All Together | 286 |
Glossary of Acronyms Terms and Abbreviations | 295 |
Index | 297 |
Citi izdevumi - Skatīt visu
Quality Assurance in the Analytical Chemistry Laboratory D. Brynn Hibbert Ierobežota priekšskatīšana - 2007 |
Quality Assurance in the Analytical Chemistry Laboratory D. Brynn Hibbert Priekšskatījums nav pieejams - 2007 |
Quality Assurance for the Analytical Chemistry Laboratory D. Brynn Hibbert Priekšskatījums nav pieejams - 2007 |
Bieži izmantoti vārdi un frāzes
accreditation body analysis analytical chemistry analytical measurements ANOVA assess bias BIPM calculated calibration cause-and-effect diagram certified reference material changes chapter chart client compared concentration confidence interval contrast coefficients control limit CuSum dard defined degrees of freedom documented equation error estimate ethanol EURACHEM example expanded uncertainty experimental design experiments factor figure give Horwitz instrument interlaboratory study International Organization ISO/IEC kilogram laboratory linear main effects mass matrix measurand measurement procedure measurement result measurement uncertainty ment method validation metrological reference metrological traceability normal distribution optimization Organization for Standardization outliers parameters performed pipette plot potassium hydrogen phthalate probability proficiency testing quality assurance quality control quality system quantity value random range Rankit repeatability replicates reproducibility requirements response sample Shewhart significant solution spreadsheet standard deviation statistical Subsection surement Table tainty temperature test material tion traceability chain uncer uncertainty components variable variance zero
Populāri fragmenti
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