Principles and Practices of Method ValidationAleš Fajgelj, Árpád Ambrus Royal Society of Chemistry, 2000 - 305 lappuses Principles and Practices of Method Validation is an overview of the most recent approaches used for method validation in cases when a large number of analytes are determined from a single aliquot and where a larege number of samples are to be analysed.Much of the content relates to the validation of new methods for pesticide residue analysis in foodstuffs and water but the principles can be applied to other similar fields of analysis. Different chromatographic methods are discussed, including estimation of various effects, eg. matrix-induced effects and the influence of the equipment set-up. The methods used for routine purposes and the validation of analytical data in the research and development environment are documented. The legislation covering the EU-Guidance on residue analytical methods, an extensive review of the existing in-house method validation documentation and guidelines for single-laboratory validation of analytical methods for trace-level concentrations of organic chemicals are also included.With contributions from experts in the field, any practising analyst dealing with method validation will find the examples presented in this book a useful source of technical information |
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1.–5. rezultāts no 57.
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... Guidelines for Single - Laboratory Validation of Analytical Methods for Trace - level Concentrations of Organic Chemicals 179 A Critique on Available In - House Method Validation Documentation 253 P. Willets and R. Wood Subject Index ...
... Guidelines for Single - Laboratory Validation of Analytical Methods for Trace - level Concentrations of Organic Chemicals 179 A Critique on Available In - House Method Validation Documentation 253 P. Willets and R. Wood Subject Index ...
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The Potential Use of Quality Control Data to Validate Pesticide Residue | 1 |
Validation of Analytical Data in a Research and Development Environment | 19 |
Effects of Sample Processing on Pesticide Residues in Fruit and Vegetables | 41 |
Testing the Effect of Sample Processing and Storage on the Stability of Residues | 75 |
AOAC International Collaborative Study on the Determination of Pesticide | 89 |
Validation of a Multiresidue Method for Analysis of Pesticides in Fruit | 108 |
Development and Validation of a Generic Gas Chromatographic Method | 120 |
Validation of Gas Chromatographic Databases for Qualitative Identification | 128 |
Estimation of Significance of Matrixinduced Chromatographic Effects | 138 |
Worked Example for Validation of a Multiresidue Method | 157 |
EU Guidance Documents on Residue Analytical Methods | 176 |
A Critique on Available InHouse Method Validation Documentation | 253 |
297 | |
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acceptable Ambrus analysis analyte concentration analytical methods analytical portions AOAC AOAC International apple applied average recovery Azinphos-methyl blank samples calculated calibration levels calibration points chemical Chlorothalonil chlorpyrifos chopper chromatographic Codex Alimentarius Codex Level coefficient collaborative study column compounds criteria CV typ CVA Q CVA detector determined Diazinon Dimethoate Endosulfan estimated ethyl acetate extraction fortification levels fortified gas chromatographic GC/MS Guidelines homogeneity homogenisation injection Iprodione isooctane kiwifruit lettuce limit of detection Lindane linear matrix effect matrix equivalent measured Methamidophos method performance method validation mg/kg obtained parameters peak performance characteristics Permethrin pesticide residues precision procedure Propargite protocol Q CVA Q quantitative range reference material regression relative standard deviation replicate reported representative analytes response retention sample processing sampling constant selected solvent specific spiked stability t-test Table tomato trueness typical uncertainty of sample values variance veterinary drug vinclozolin
Atsauces uz šo grāmatu
Handbook of Elemental Speciation: Techniques and Methodology, 1. sējums Joseph A. Caruso,Helen Crews,Klaus G. Heumann Ierobežota priekšskatīšana - 2003 |
Analysis of Pesticides in Food and Environmental Samples Jose L. Tadeo Ierobežota priekšskatīšana - 2008 |